Superplastic Properties of Ultrafine-Grained AA6061 Alloy Fabricated by Cyclic Expansion-Extrusion
DOI:
https://doi.org/10.3849/aimt.02075Keywords:
AA6061 aluminum alloy, ; cyclic expansion-extrusion, ultrafine grains, severe plastic deformation, superplastic properties, superplastic formingAbstract
This paper investigates the superplastic behavior of AA6061 aluminum alloy processed by cyclic expansion-extrusion, a severe plastic deformation method producing ultrafine-grained structures. Cylindrical specimens underwent up to four cyclic expansion–extrusion cycles at room temperature. The average grain size decreased from ~100 μm (annealed state) to 5–6 μm after four cycles, with nearly 75 % higher and more homogeneous microhardness. The refined microstructure fulfils conditions for superplasticity dominated by grain boundary sliding at elevated temperatures. Tensile tests showed a maximum elongation of ~330 % at 530 °C and strain rate 10−3s−1, with a low maximum flow stress of 9.5 MPa. The results confirm cyclic expansion–extrusion as an effective route to enhance microhardness and enable superplastic forming of lightweight AA6061 alloys.
References
SUN, Y. The Use of Aluminum Alloys in Structures: Review and Outlook Structures, 2023, 57, 105290. https://doi.org/10.1016/j.istruc.2023.105290.
KHALAFE, W.H., E.L. SHENG, M.R.B. ISA and S.B. SHAMSUDIN. Enhancing Mechanical Characteristics of 6061‑T6 with 5083‑H111 Aluminium Alloy Dissimilar Weldments: A New Pin Tool Design for Friction Stir Welding (FSW). Metals, 2024, 14(5), 534. https://doi.org/10.3390/met14050534.
LUO, Z., X. ZHANG, Z. LIU, H. ZHOU, M. WANG and G. XIE. Mechanical Properties and Interfacial Characteristics of 6061 Al Alloy Plates Fabricated by Hot‑Roll Bonding. International Journal of Minerals, Metallurgy and Materi-als, 2024, 31, pp. 1890-1899. https://doi.org/10.1007/s12613-023-2801-8.
HUANG, Y. and T.G. LANGDON. Advances in Ultrafine-Grained Materials. Materials Today, 2013, 16(3), pp. 85-93. https://doi.org/10.1016/j.mattod.2013.03.004.
EDALATI, K., et al. Nanomaterials by Severe Plastic Deformation: Review of Historical Developments and Recent Advances. Materials Research Letters, 2022, 10(4), pp. 163-256. https://doi.org/10.1080/21663831.2022.2029779.
NGUYEN, Q.C., D. OLASZ, A.Q. AHMED, E.V. BOBRUK and R.Z. VALIEV. Review on Grain Size- and Grain Boundary Phenomenon in Unusual Mechani-cal Behavior of Ultrafine-Grained Al Alloys. Materials Transactions, 2023, 64(8), pp. 1844-1855. https://doi.org/10.2320/matertrans.MT-MF2022020.
LAPLANCHE, G., T. HIGASHI and M.J. STARINK. Grain Boundary Sliding and Strain Rate Sensitivity of Coarse and Fine/Ultrafine Grained 5083 Aluminum Alloys. Metallurgical and Materials Transactions A, 2020, 51(1), pp. 1109-1122. https://doi.org/10.1007/s11661-019-05583-5.
KWEITSU, E.K., D.K. SARKAR and X.-G. CHEN. A Short Review on Super-plasticity of Aluminum Alloys. Engineering Proceedings, 2023, 43(1), 43. https://doi.org/10.3390/engproc2023043043.
BHATTA, L., A. PESIN, A.P. ZHILYAEV, P. TANDON, C. KONG and H. YU. Recent Development of Superplasticity in Aluminum Alloys: A Review. Met-als, 2020, 10(1), 77. https://doi.org/10.3390/met10010077.
BOBRUK, E.V., N.G. ZARIPOV, I.A. RAMAZANOV, N.Q. CHINH and R.Z. VALIEV. Low-Temperature Superplasticity of Ultrafine-Grained Aluminum AAlloys: Recent Discoveries and Innovative Potential. Materials, 2024, 17(13), 3311. https://doi.org/10.3390/ma17133311.
ZRNÍK, J., S.V. DOBATKIN and I. MAMUZI. Processing of Metals by Severe Plastic Deformation (SPD) – Structure and Mechanical Properties Respond. Metalurgija, 2008, 47(3), pp. 211-216. ISSN 0543-5846.
VALIEV, R.Z., R.K. ISLAMGALIEV and I.V. ALEXANDROV. Bulk Nanostruc-tured Materials from Severe Plastic Deformation. Progress in Materials Science, 2000, 45(2), pp. 103-189. https://doi.org/10.1016/S0079-6425(99)00007-9.
LI, X., M. DU, Z. MAO, T. HUANG and C. BAN. Recent Advances in the Equal Channel Angular Pressing of Metallic Materials. Processes, 2022, 10(11), 2181. https://doi.org/10.3390/pr10112181.
ZHILYAEV, A.P. and T.G. LANGDON. Using High-Pressure Torsion for Metal Processing: Fundamentals and Applications. Progress in Materials Science, 2008, 53(6), pp. 893-979. https://doi.org/10.1016/j.pmatsci.2008.03.002.
NGUYEN, M.T., V.T. LE, M.H. LE and T.A. NGUYEN. Superplastic Properties in a Ti5Al3Mo1.5V Titanium Alloy Processed by Multidirectional Forging Process. Materials Letters, 2022, 307, 131004. https://doi.org/10.1016/j.matlet.2021.131004.
RICHERT, M., H. PETRYK and S. STUPKIEWICZ. Grain Refinement in AlMg-Si Alloy during Cyclic Extrusion–Compression: Experiment and Modelling. Archives of Metallurgy and Materials, 2007, 52(1), pp. 49-54. ISSN 1733-3490.
PARDIS, N., B. TALEBANPOUR, R. EBRAHIMI and Z. ZOMORODIAN. Cyclic Expansion–Extrusion (CEE): A Modified Counterpart of Cyclic Extrusion–Compression (CEC). Materials Science and Engineering A, 2011, 528, pp. 7537-7540. https://doi.org/10.1016/j.msea.2011.06.059.
KRATOCHVÍL, J. Mechanism of Grain Refinement Induced by Severe Plastic Deformation. Materials Science Forum, 2010, 667-669, pp. 617-622. https://doi.org/10.4028/www.scientific.net/MSF.667-669.617.
TRUONG, D.X., M.T. NGUYEN, M.H. NGUYEN and T.A. NGUYEN. Effect of the Cyclic Expansion–Extrusion Process on Mechanical Properties and the Grain Refinement of AA6061 Aluminum Alloy. Journal of Military Science and Technology, 2023, 87, pp. 100-107. https://doi.org/10.54939/1859-1043.j.mst.87.2023.100-107.
NGUYEN, M.T. Experimental Determination of Process Parameters for Super-plastic Forming from AA7075 Aluminum Alloy [online]. Suranaree Journal of Science and Technology, 2022, 29(5), 010163(1-6) [viewed 2025-11-09]. Available from: https://ird.sut.ac.th/e-journal/Journal/pdf/220104793.pdf
KAIBYSHEV, R., F. MUSIN and D.R. LESUER. Superplasticity in Al–Mg–Sc–Zr Alloys Processed by Equal-Channel Angular Pressing. Acta Materialia, 2005, 53(15), pp. 4053-4064. https://doi.org/10.1016/j.actamat.2005.05.020.
XU, C., Z. HORITA and T.G. LANGDON. Superplasticity in an Al–Cu Alloy Processed by Equal-Channel Angular Pressing. Acta Materialia, 2008, 56(6), pp. 1435-1446. https://doi.org/10.1016/j.actamat.2007.12.007.
NGUYEN, M.T. and T.A. NGUYEN. Microstructure and Microhardness of AA6061 Aluminum Alloy Formed by Cyclic Expansion–Extrusion Process:Numerical Simulation and Experimental Evaluation. Archives of Metallurgy and Materials, 2025, 70(2), pp. 625-632. https://doi.org/10.24425/amm.2025.153463.
BACCA, M., D.R. HAYHURST and R.M. MCMEEKING. Continuous Dynamic Recrystallization during Severe Plastic Deformation. Mechanics of Materials, 2015, 90, pp. 148-156. https://doi.org/10.1016/j.mechmat.2015.05.008.
YANG, Q., T. WOJCIK and E. KOZESCHNIK. Continuous Dynamic Recrystallization and Deformation Behavior of an AA1050 Aluminum Alloy during High-Temperature Compression. Metals, 2024, 14(8), 889. https://doi.org/10.3390/met14080889.
KAIBYSHEV, R., A. GOLOBORODKO, F. MUSIN, I. NIKULIN and T. SAKAI. The Role of Grain Boundary Sliding in Microstructural Evolution during Superplastic Deformation of a 7055 Aluminum Alloy. Materials Transactions, 2002, 43(10), pp. 2408-2414. https://doi.org/10.2320/matertrans.43.2408.
KUZNETSOV, A., L. KARKINA, Y. GORNOSTYREV and P. KORZHAVYI. Effects of Zn and Mg Segregations on the Grain Boundary Sliding and Cohe-sion in Al: Ab Initio Modelling. Metals, 2021, 11(4), 631. https://doi.org/10.3390/met11040631.
YAKOVTSEVA, O., M. SITKINA, A.O. MOSLEH and A. MIKHAY-LOVSKAYA. High Strain Rate Superplasticity in Al–Zn–Mg-Based Alloy: Mi-crostructural Design, Deformation Behavior, and Modeling. Materials, 2020, 13(9), 2098. https://doi.org/10.3390/ma13092098.
LEE, S., K. WATANABE, K. MATSUDA and Z. HORITA. Low-Temperature and High-Strain-Rate Superplasticity of Ultrafine-Grained A7075 Processed by High-Pressure Torsion. Materials Transactions, 2018, 59(8), pp. 1341-1347. https://doi.org/10.2320/matertrans.L-M2018825.
Downloads
Published
License
Copyright (c) 2026 Advances in Military Technology

This work is licensed under a Creative Commons Attribution-NonCommercial 4.0 International License.
Authors who publish with this journal agree to the following terms:
1. Authors retain copyright and grant the journal right of first publication with the work simultaneously licensed under a Creative Commons Attribution License that allows others to share the work with an acknowledgement of the work's authorship and initial publication in this journal.
2. Authors are able to enter into separate, additional contractual arrangements for the non-exclusive distribution of the journal's published version of the work (e.g., post it to an institutional repository or publish it in a book), with an acknowledgement of its initial publication in this journal.
3. Authors are permitted and encouraged to post their work online (e.g., in institutional repositories or on their website) prior to and during the submission process, as it can lead to productive exchanges, as well as earlier and greater citation of published work.
Users can use, reuse and build upon the material published in the journal for any purpose, even commercially.



